The following table gives an overview of the techniques available at ELMICAU and the corresponding properties they can measure, alongside the best resolution that can be reached. 

 

 

elemental

composition

morphology surface topology magnetic structure chemical map crystalline structure special
2D 3D 2D 3D
TEM imaging    

< 0.1 nm

          strain/stress
TEM/STEM diffraction               < 1 nm  
TEM Lorentz mode           < 10 nm      

HAADF

(STEM)

    < 0.1 nm            
EELS (TEM/STEM) < 0.1 nm           < 0.1 nm    
EDX (TEM/STEM) < 0.1 nm                
HRSTEM imaging     < 0.1 nm         < 0.1 nm  
DPC (STEM)           < 10 nm    

E-fields: 

< 0,1 nm

Lorentz-STEM (Cs-corrected)           < 1 nm      
SE (SEM)         < 5 nm       large-scale images possible
BSE (SEM) < 10 nm              
EDX (SEM) < 50 nm              
EBSD (SEM)               < 20 nm grain orientation
Auger (AES) < 5 nm                
TEM/STEM tomography   < 10 nm   < 10 nm          
FIB tomography   < 100 nm   < 100 nm          
Auger tomography   < 5 nm  

< 5 nm

         

 

                Elemental composition: differentiation between different elements.

                Morphology: the physical texture of the sample, i.e. granular, single-crystalline, amorphous, etc. 

                Surface topology: the texture of the sample surface.

                Magnetic structure: magnetic domains or domain walls, spin structures like vortices or skyrmions.

                Chemical map: differentiation between different elements and their chemical state, e.g. different oxidation levels.

                Crystalline structure: Bravais lattice and lattice constants.

 

This table can be used to find a suitable technique for inquiry regarding certain properties. However, the list is not exhaustive, and conversation with the professional ELMICAU staff is still the best way for finding the right technique for your situation.

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